University of Calabria
University of Calabria
Italian English

LCM – Material Characterization Lab

immagine LCM STAR

The Materials Characterization Laboratory (MCL) offers a wide range of services for the mechanical and thermal analysis of materials used in scientific and technological applications.

With modern equipment and measurement techniques, the lab can analyze components and samples, even under simulated operating conditions, using both traditional and advanced structural and functional materials. Temperature-controlled testing can be performed to assess both global and local material properties. The lab is also equipped with non-destructive diagnostic methods, utilizing both point-based and full-field techniques.

The current research focuses on investigating fracture mechanisms in metallic, ceramic, polymeric, and composite materials—both traditional and innovative—relevant to engineering and biomedical applications. This is achieved by analyzing tomographic reconstructions of the material’s interior and the three-dimensional strain field around defects, notches, interfaces, and joints, even in-line and in real-time, downstream of the high-energy Materia beamline. The study explores the nucleation and propagation of defects in metallic materials under fatigue loading while also identifying the three-dimensional shapes that cracks can develop when subjected to mechanical loads.

The research also explores the mechanisms governing creep in polymeric materials, the distribution of defects and voids in ceramics and polymers, and the various failure modes of composite materials. This includes analyzing the interactions between intralaminar failures caused by matrix cracking, fiber breakage, fiber pull-out, and delamination phenomena resulting from impact events.

High-energy impact tests, conducted using the existing drop tower, will be used to validate current empirical and semi-empirical models and, if necessary, to develop new models for analyzing the fracture behavior of composite materials.

With the volumetric image analysis software currently being acquired, displacement and strain fields within mechanically loaded samples will be measured, along with the three-dimensional surface displacement field. This will be achieved by analyzing images captured using a 3D digital decorrelation system also in the process of acquisition. Measurements taken near notches, holes, and annular cuts—introduced to relieve residual stresses in the material—can be used to develop methods for measuring the three-dimensional distribution of internal stresses.

Finally, the matter metrology room will be set up and put into operation, enabling the study of material surface structures at the microscopic level, the execution of vibro-acoustic measurements, and the provision of calibration services for instruments measuring mass, dimensions, and temperature.

2025
Nicoletti, F., Arcuri, N. · A new methodology for the in-situ measurement of thermal transmittance and thermal capacity of opaque walls: Thermal Decoupling Method (TDM). Building and Environment, 276, 112881 (2025). DOI 10.1016/J.BUILDENV.2025.112881
2024
Garofalo F., Rovale R., Morano C. et al. · On the fatigue behaviour of epoxy-based nanostructured composite materials · Journal of Reinforced Plastics & Composites (in press) DOI 10.1177/07316844241244499 
Rotella G., Morano C. et al. · Surface functionalization of titanium screws for orthopaedic implant applications · CIRP Annals 73 (1): 453-456 (2024)
Morano C., Scagliola M. et al. · Crack propagation in adhesive-bonded 3-D-printed polyamide: surface vs bulk patterning · Int. J. Adhesion & Adhesives 131: 103660 (2024)
2023
Morano C., Wagih A. et al. · Improving performance of composite/metal T-joints by corrugated aluminium stiffeners · Composite Structures 307 (2023)
Morano C., Terasaki N. et al. · Snap-through crack propagation in architected bonded interfaces analysed via mechanoluminescent coating · ACS Appl. Mater. & Interfaces 15: 40887-40897  (2023)
Morano C., Alfano M., Pagnotta L. · Effect of strain-rate and heat exposure on PA12 processed via SLS · Materials 16 (2023) 
Morano C., Crocco P. et al. · Porosity evolution in PA12 SLS parts studied by µ-CT · Int. J. Adv. Manuf. Technol. 125: 3229-3240  (2023)
Bruno, R., Bevilacqua, P. · Bio-PCM to enhance dynamic thermal properties of dry-assembled wooden walls: Experimental results. Building and Environment. 242, 110526 (2023)
2022
Morano C., Tao R., Alfano M. et al. · Toughening effect in CFRP/AA corrugated adhesive joints · Materials Today Communications 32 (2022)
Bruno, R.; Bevilacqua, P.; Rollo, A.; Barreca, F.; Arcuri, N. · A Novel Bio-Architectural Temporary Housing Designed for the Mediterranean Area: Theoretical and Experimental Analysis. · Energies 15, 3243 (2022)
2021
Renzo D.A., Sgambitterra E., Maletta C. et al. · Multiaxial fatigue behaviour of SLM Ti-6Al-4V · Fatigue & Fracture Eng. Mater. Struct. 44: 2625-2642 (2021)
Bruno, R., Bevilacqua, P., Ferraro, V., Arcuri, N.· Reflective thermal insulation in non- ventilated air-gaps: experimental and theoretical evaluations on the global heat transfer coefficient. Energy and Buildings, 236, 110769. DOI 10.1016/J.ENBUILD.2021.110769 (2021)
Carraturo M., Alaimo G. et al. · 3-D-printed 316L lattice structures: experiments & FEM · J. Mater. Eng. Perf. 30: 5247-5251 (2021)
Sgambitterra E., Magarò P. et al. · Fatigue crack growth in austenitic/martensitic NiTi · Shape Memory & Superelasticity 7: 250-261  (2021)
Sgambitterra E., Niccoli F. · Inverse problems with digital image correlation · Frattura ed Integrità Strutturale 57: 300-320  (2021)
Sanguedolce M., Zekonyte J., Alfano M. · Wear of 17-4 PH SLM patterned surfaces · Applied Sciences 11: 9317  (2021)
Morano C., Tao R. et al. · Effect of mechanical pretreatments on CFRP/epoxy joints · Materials 14: 1512  (2021)
Frascio M., Mandolfino C. et al. · Surface preparation in AM adhesive bonding · Int. J. Adhesion & Adhesives 106  (2021)
2020
Morano C., Zavattieri P., Alfano M. · Tuning energy dissipation in bio-inspired interfaces · J. Mech. Phys. Solids 141: 103965 (2020)
Furgiuele F., Magarò P. et al. · Functional & structural fatigue of pseudoelastic NiTi · Shape Memory & Superelasticity 6: 242-255 (2020)
Palumbo G., Piccininni A. et al. · Custom titanium cranial prostheses: manufacturing & drop-test FEM · Int. J. Adv. Manuf. Technol. 111: 1627-1641 (2020)
2019
Magarò P., Marino A.L. et al. · Stellite-6 coatings by cold-spray · Surf. & Coat. Technol. 377: 124934 (2019)
Sgambitterra E., Maletta C. et al. · Strain-life fatigue of pseudoelastic NiTi · Smart Mater. & Struct. 28 (2019)
Sgambitterra E., Maletta C. et al. · Temperature effects on NiTi fatigue crack propagation · Shape Memory & Superelasticity 5: 278-291 (2019)
Corigliano P., Crupi V. et al. · Fatigue of Ti-6Al-4V laser-welded joints · Frattura ed Integrità Strutturale 43: 171-181 (2019)
Morano C., Musiari F. et al. · Automotive hot-setting adhesives in steel joints · J. Mater. Design & Appl. 233 (10): 2084-2093 (2019)
2018
Magarò P., Marino A.L. et al. · Wear-resistant coatings by cold spray · Proc. Struct. Integr. 9: 287-294 (2018)
Bruno, R., Bevilacqua, P., Cuconati, G., & Arcuri, N. · An innovative compact facility for the measurement of the thermal properties of building materials: first experimental results. · Applied Thermal Engineering. 143, 947–954 (2018)
Lamuta C., Campi D. et al. · Mechanical properties of SnSe semiconductor · J. Phys. Chem. Solids 116: 306-312 (2018)
Bruno L. · Nanometric 3-D displacement by digital profile correlation · Materials & Design 159: 170-185 (2018)
Bruno L. · Confocal microscopy + DIC for 3-D vectors · Proc. Struct. Integr. 12: 567-577 (2018)
Alfano M., Bruno L., Morano C. et al. · Debonding in AM bio-inspired interfaces · Proc. Struct. Integr. 8: 604-609 (2018)
Morano C., Bruno L. et al. · Crack trapping in 3-D-printed bio-interfaces · Proc. Struct. Integr. 12: 561-566 (2018)
Sgambitterra E., Lamuta C. et al. · Brazilian disk test & DIC on brittle materials · Materials & Structures 51 (2018)
2017
Niccoli F., Garion C. et al. · Beam-pipe coupling with SMA rings · Materials & Design 114: 603-611 (2017)
Maletta C., Bruno L. et al. · Fatigue damage in SMA by nanoindentation · Mater. Sci. & Eng. A 684: 335-343 (2017)
2016
Lamuta C., Cupolillo A. et al. · Nanoindentation of Bi₂Te₃ topological insulators · Phys. Status Solidi B 253: 1082-1086 (2016)
Lamuta C., Candamano S. et al. · Direct piezoelectric effect in geopolymeric mortars · Materials & Design 107: 57-64 (2016)
Lamuta C., Campi D. et al. · Bi₂Te₃ mechanical properties by DFT + indentation · Scripta Materialia 121: 50-55 (2016)
Lamuta C., Cupolillo A. et al. · Fracture toughness of Bi₂Te₃ single crystals · Nano Research 9: 1032-1042 (2016)
2015
Sgambitterra E., Lesci S. et al. · Higher-order terms in SMA fracture mechanics · Procedia Engineering 109: 457-464 (2015)
Sgambitterra E., Maletta C. et al. · Local phase transformation in NiTi by nanoindentation · Scripta Materialia 101: 64-67 (2015)
Maletta C., Niccoli F. et al. · Stress-induced martensite at crack tips in NiTi · Frattura ed Integrità Strutturale 30: 167-173 (2015)
Sgambitterra E., Maletta C. et al. · Crack-tip transformation in NiTi alloys · Shape Memory & Superelasticity 1: 275-283 (2015)
Rotella G., Alfano M. et al. · Pulsed Yb-laser surface modification of Ti-6Al-4V · CIRP Annals 64: 527-530 (2015)
Lamuta C., Di Girolamo G., Pagnotta L. · Nanostructured YSZ coatings by APS · Ceramics International 41: 8904-8914 (2015)
2014
Maletta C., Bruno L. et al. · Crack-tip thermal & mechanical hysteresis in SMA under fatigue · Mater. Sci. & Eng. A 616: 281-287 (2014)